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Both hyphenated techniques provide baseline separation of the four deoxynucleotide monophosphates (d NMP), which are present in the DNA chain.
With CE-ICP-MS, detection limits for phosphorus down to 53 µg L (2´ -deoxythymidine-5´ -monophosphate, d TMP) (corresponding to 0.03 ng P absolute) were obtained.
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The chamber pressure was maintained in the range of a few Torr, which also influenced system optimization.
A narrow central channel was formed inside the plasma when the aerosol gas flowed, and atomic emission was observed at the end-on side of the plasma.
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